Press Release

Jamshedpur: 26th November, 2008

 

National Metallurgical Laboratory, Jamshedpur will be organising the VI  International Conference on Mechanochemistry and Mechanical Alloying during 1- 4 Dec, 2008. About 80 foreign delegates from 24 countries and 200 Indian delegates are expected to participate in the Conference. The INCOME series of conferences initiated by International Mechanochemistry Association [an associate member of International Union of Pure and Applied Chemists (IUPAC)] has served as a common platform to bring together all stakeholders from academia, Research and Development organisations, and industry to foster the growth of the discipline.The first international conference on ‘Mechanochemistry and Mechanical Alloying (INCOME1992)’ was held in Koásice (Slovakia) in 1992. This was followed by INCOME1997 in Novosibirsk (Russia), INCOME2000 in Prague (Czech Republic); INCOME2003, in Braunschweig (Germany), and INCOME2006 again in Novosibirsk. This is the first time that a conference of INCOME repute is going to be held in India, and in Jamshedpur. Dr. T. Ramasami, Secretary, Department of Science & Technology, Govt. of India will be the chief guest. Prof. M. Senna, President , International Mechanochemistry Association will give the conference lecture. In addition to presentation of technical papers, scientific posters will be displayed. An exhibition has also been also organized where state of the art milling devices and characterization equipments will be displayed.

 

 Mechanochemistry and mechanical activation have moved a long way and have evolved as frontier areas of research and applications, during the last two to three decades. Notable developments have taken place in terms of scientific understanding and applications in diverse fields, encompassing all facets of metallurgy including metal extraction, alloying, composites; traditional and advanced ceramics processing; paints, pigments and dyes; catalysis, pharmaceuticals, agriculture, utilization of wastes, energy and environment, and many more. Simultaneous developments have taken place in terms of characterization techniques of activated solids; quantification and control of activation processes; and mechanical activation devices for specific needs, etc. The developments in the field of mechanochemistry are unfolding at a rapid rate in terms of basic science, range of applications, and their impact. While significant advances are taking place in each of the application areas, e.g. smart mechanochemistry, pharmaceuticals, etc., and call for periodic review, the need for cross fertilization of concepts and ideas is increasingly becoming apparent. The four day deliverables will contain all facets of Mechanochemistry including basic science, application to various areas, newer developments and devices, and industrial applications.

 

 

Jamshedpur, 1st December 2008

 

The Inaugural function of the VIth International Conference on Mechanochemistry and Mechanical Alloying (INCOME 2008) was organized by NML, Jamshedpur today. Dr. T. Ramasami, Secretary, Department of Science and Technology, Govt. of India was the Chief Guest of the ceremony. About 200 delegates including 60 foreign scientists and researchers are participating in the conference.

 

Prof. S. P. Mehrotra, Director, National Metallurgical Laboratory and Chairman, INCOME 2008 welcomed all the delegates. He mentioned that Mechanochemistry is an evolving discipline and talked about its fundamentals, widening of applications and the newer equipment and devices used for the purpose. In the presidential address Prof. Peter Balaz, founding member of the International Mechanochemistry Association highlighted the history of the International Mechanochemistry Association, which was founded in 1988.

 

Dr. T. Ramasami, Secretary, Department of Science and Technology, Govt. of India delivered a talk on ‘Revealing Beauty and Wonders of Nano World’. He said that Nature has employed several principles of mechano-chemistry and nano- size materials and structures had always existed. Our realization of the behavior of materials of nano size that has excited the world and global expectations are very high. He also talked upon the beauty and wonders of nano structures in collagen. The natural nano sized structures like skin for perspiration and transpiration, peacock feather for decoration and shells, bones for protection and load bearing functions are yet to be replicated by man kind.

 

Dr. Rakesh Kumar, Convenor, INCOME 2008 proffered the vote of thanks at the conclusion of the ceremony

 

 

Jamshedpur,  2nd December 2008

 

The second day of INCOME 2008 included sessions in Mechanochemistry of Macromolecules and Applications in Pharmaceuticals, Severe Plastic Deformation and Friction Stir Welding, Mechanical Alloying and Advanced Materials, Building Management and Environment Management and Nano- Particles and Nano- Composites. The sessions were preceded by the Plenary Session Special Lectures. A total number of 29 papers presented today.  About 167 delegates including 47 foreign scientists and researchers had participated in the today’s session.

 

The sessions of today were preceded by three Plenary Lectures: “Ultrafine grained materials through mechanical processing: An overview” presented by, Prof. K.A. Padmanabhan, Anna University,  “Mechanochemistry of macromolecules and applications to pharmaceuticals: where are we now? “ presented by Dr. E. Boldyreva, ” Using mechanical properties of crystals to quantify intermolecular interactions” presented by, Prof. G. R. Desiraju, University of Hyderabad. Some of the other important papers were presented in today’s sessions were as follows:

 

Dr. Ashwini Nangia, University of Hyderabad presented  “Cocrystal design for pharmaceutical forms”. He presented various  aspects of pharmaceutical cocrystals and polymorphs  e.g.  development of new heterosynthons using strong hydrogen bond recognition and selective pairing of donors and acceptors. Dr. C. Malla Reddy,  Indian Institute of Science Education and Research, kolkata  presented “ Structure–property correlations in shearing, bending and brittle organic crystals”.  Dr.K.G. Korolev, Institute of Solid State Chemistry, Russia presented paper “Cell wall transformation during mechanical activation”. Prof. Indranil Manna,  IIT, Kharagpur delivered a talk on  “Mechano-chemical synthesis of Al-based nanocrystalline/ amorphous alloys for high specific strength applications”   He threw light on his current study  devoted to  synthesize Al65Cu20Ti15 and Al50Ti40Si10 alloys with in-situ nanometric intermetallic precipitates and/or nano-oxide (TiO2) dispersion by solid-state mechanical alloying route and consolidate milled powder by different sintering methods. Dr. M. Besterci , Institute of Materials Research of Slovak Academy of Sciences, Kosice, Slovak Republic delivered a talk on Mechanical alloying of Al-C system. Dr. K. L. Murty, North Carolina State University, USA presented   “Creep behavior of ball-milled nanocrystalline aluminum”. Dr. Debasish Bhattacharjee, Tata Steel, Jamshedpur  presented ”Nanofluids as coolants: Applications in steel industries”. Dr. A.N. Streletskii, N. N. Semenov Institute of Chemical Physics, Moscow presented  “Metal- oxidizer mechanoactivated energetic nano composites" Kang-In Rhee, Resource Recycling R&D Centre, Korea presented "Recycling R&D program at the RRDC Korea”  

 

A poster session  was organized today where about 35 posters were presented

 

 

 

Jamshedpur,  3rd December 2008

 

A total number of 28 papers were presented on the third day of the VI International Conference on Mechanochemistry and Mechanical Alloying (INCOME 2008) .  Today’s sessions included papers in the areas of Mechanochemistry of Macromolecules and Applications in Pharmaceuticals, Advance Ceramics Science and Technology, Mechanical Alloying and Advanced Materials, Mineral Processing and Extractive Metallurgy. The sessions were preceded by the Plenary Session Special Lectures. “Plastic deformation of fully dense Nanocrystalline material” presented by, Dr. H. J. Fecht, Werkstoffe der Elektrotechnik, Universität Ulm Germany, “On the existence of dynamic critical points“ presented by Dr. J. Linol, Université de Rouen,  France, ”Estimation of mechanochemical effects in heterogeneous processes”, presented by, Dr. G. Mulas, Universitŕ di Sassari, Italy.  Some of the important papers presented in today’s sessions are as following:

 

 Dr. T. P. Shakhtshneider, Institute of Solid State Chemistry and Mechanochemistry, Russia, presented “Mechanochemistry and solubilization of drugs”. He explained about his dissolution studies showing that in the case of mechanocomposites, the release rate and solubility of meloxicam increased compared with those of the physical mixtures of the components and pure crystalline drug. This study will be potentially useful in improving the oral bioavailability of poorly water-soluble drugs.  Dr. T. T. Friščić, University of Cambridge, Cambridge presented the paper “Development of liquid- assisted grinding for the synthesis of hydrogen-bonded and coordination frameworks”. He highlighted that the application of mechanosynthesis to the construction of non-covalent e.g. hydrogen or halogen bonds between molecules has been significantly improved by introducing a small amount of a liquid phase into the mechanochemical reaction mixture. He also talked about the recent discovery of molecular templating during LAG, which has added an additional level of control to mechanochemical synthesis of soft materials. The talk delivered by Dr. B. S. Murty, Indian Institute of Technology, Chennai, threw light on high energy ball milling that has established itself as a viable and versatile route for the synthesis of nano materials. His presentation dealt with the synthesis and properties of nano materials prepared by high energy ball milling.  Dr. N. K. Mukhopadhyay, Banaras Hindu University, Varanasi, presented “Synthesis of Nanocrystalline and amorphous phases in complex metallic alloys during mechanical miling”. He said about the Metal matrix composite (MMC) technology, which significantly improves the wear resistance, elastic modulus and tensile strength of unreinforced metals and alloys. In his paper a novel and cost-effective processing route for in situ synthesis of TiC particulates utilizing the self-propagating high-temperature synthesis reaction of Al–Ti–C performs in molten magnesium was investigated.

 

 Dr. N. Kosenko, Ivanovo State University of Chemical Technology, Russia, presented “The mechanical treatment as a method of substances passivation”, Dr. A. Politov, Institute of Solid State Chemistry and Mechanochemistry SB RAS, Novosibirsk presented “Dimerization of anthracene and relatedsubstances in diamond anvils and glass mill”,  Dr. Sh.Raygan, University of Tehran presented “Effect of mechanical activation on the in-situ production of Fe-TiC composite”,  Dr. Projjal Basu, Universiti Sains Malaysia, Malaysia presented “Synthesis of nanostructured titanium carbide from Titanium oxide and Ferrotitanium through mechanical activation”,  Dr. T. Mousavi, Isfahan University of Technology, Iran presented “The effect of Al2O3 content on the formation mechanism and properties of NiTi-Al2O3 nano composite synthesized by mechanical alloying”,  Dr. Bassin Marc, Thermo Fisher Scientific SARL, Switzerland presented the paper “Integrated automation solutions for top analytical performance and maximum efficiency”,   Dr. M.S. Senthil Saravanan, National Institute of Technology, Tiruchirappalli presentedInfluence of micro and nanocrystalline powdermatrix on mechanical properties of CNT reinforced Al-matrix composites,  Dr. N. Kosova, Institute of Solid State Chemistry and Mechanochemistry SB RAS,  Novosibirs  presentedNew composite ‘nano-micro’ cathode materials for lithium-ion batteries prepared via mechanochemical route”,  Dr. T.Rojac  Jozef Stefan Institute, Ljubljana, presented  “Mechanochemical synthesis of NaNbO3: a study of the reaction mechanism”,  Dr. I. Konstanchuk, Institute of Sold State Chemistry and Mechanochemistry, Russia, presented  “ Mechanically alloyed magnesium-based materials for hydrogen storage and Dr. O.S. Morozova, Institute of Chemical Physics RAS, Russia, presented “Stimulating effect of boron admixture on hydrogen sorption-desorption properties of mechanically activated Titanium”.

 

Some other important invited papers presented in today’s session were “Mechanochemical reactions of clay minerals with CsCI” presented by Dr. S. Yariv, the Hebrew University of Jerusalem, Jerusalem, ”Theoretical and application aspects concerning material treatment in the Dynamic type mills” by Dr. T. A. Ketegenov, National Engineering Academy of the Republic of Kazakhstan, Kazakhstan.  

 

 In the poster session about 35 posters were presented.

 

 

 

Jamshedpur,  4th December 2008

The fourth day of the VIth International Conference On Mechanochemistry and Mechanical Alloying (INCOME 2008) included sessions in Mechanical Alloying and Advanced Materials, and Advance Ceramics Science and Technology. The sessions were preceded by the Plenary Session Special Lectures. A total number of 11 papers were presented today. The sessions of today were preceded by three Plenary Lectures: “Glass formation” presented by, Prof.P.Ramachandra Rao,  “Local structure and size- dependent properties of nanooxides prepared by mechanochemical routes“ presented by Dr. V. Šepelák, Braunschweig University of Technology, Germany , and ” Specifics of mechanically driven atomic distributions in interstitial alloys” presented by, Dr. J. Foct, Université de Lille. Some of the important papers presented in today’s sessions are as follows:

Dr. S. Srikanth, National Metallurgical Laboratory Madras Centre, Chennai presented “Where does the energy go in high energy milling?. He highlighted that for understanding the magnitude and timescales of the temperature rise during the high energy milling process, a study was undertaken using low melting metals and alloys. The experimentally determined crystallite size and strain correlated well with the values estimated from line broadening analysis. Conversely, the experimental melting point depression due to strain correlated well with the theoretical calculations. Dr. P.C. Angelo, PSG College of Technology, Coimbatore, presented “Hot isostatic pressing of yttria dispersed 9Cr martensitic steel synthesized by mechanical alloying”. He described the synthesis of ODS 9Cr Martensitic steel by Mechanical Alloying of elemental metal precursors. Nanocrystalline yttria used as the dispersoid was synthesized via an efficient and economic Sol-Gel method. Dr. S. Tikhov, Boreskov Institute of Catalysis., presented “Design of the composite porous cermets synthesized through mechanical alloying of Cr-Al powder followed by hydrothermal treatment and calcination” . He focused that the cermet monoliths have sufficiently high mechanical strength (up to ~20 MPa) and porosity (35-57 %) with large pores (1-10 mm) to be used as catalyst and membrane supports. The evolution of microstructure with the Cr-Al powder alloying time had been discussed. Dr. P.Brahma, Gurudas College,Kolkata, presented “Novel transport properties of nanostructured ferric oxide“  He highlighted that the resistivity variation of the unmilled sample can be ascribed to typical band conduction. The resistivity decreases substantially with the progress of ball milling. A decrease of about two orders of magnitude of resistivity was observed for the specimen ball milled for 10h.It is clearly observed that the resistivity variation of the Two activated processes were observed with activation energies of ~0.06 and ~0.7eV, respectively. Large and small particle sizes are responsible for the two activation energies.

 

Dr. P. P. Chattopadhyay, Bengal Engineering and Science University, Shibpur, presented “Blue-violate photoluminescence from colloidal suspension of nanocrystalline silicon-silicon oxide matrix prepared by ball milling” He said that the intense violet-blue emission from nc-Si in Si-oxide matrix prepared by chemically induced oxidation of mechanically milled Si. Si powder was used as starting materials. He also mentioned that there had been no previous report on blue PL from nc-Si prepared by ball milling. The novel and inexpensive synthesis route of nc-Si in oxide matrix, exhibiting blue-violet PL, will open up a huge scope for potential applications. Dr.  A. Radhika Devi, Indian Institute of Technology, Chennai presented “Effect of surfactant addition on magnetic properties of Fe3O4 nanoparticles by ball milling” She said that, Magnetite nano particles were synthesized in the presence of starch as surfactant by ball milling for 30 hours in toluene medium. The amount of surfactant   addition was varied (8 wt %, 9 wt %,10 wt% ,11 wt % and 12 wt %) to study the variation of structural and magnetic properties with surfactant content.

 

 

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