Jamshedpur: 26th November,
2008
National Metallurgical Laboratory, Jamshedpur will be organising the
VI International Conference on Mechanochemistry and Mechanical
Alloying during 1- 4 Dec, 2008. About 80 foreign delegates from 24
countries and 200 Indian delegates are expected to participate in
the Conference.
The INCOME series
of conferences initiated by International Mechanochemistry
Association [an associate member of International Union of Pure and
Applied Chemists (IUPAC)] has served as a common platform to bring
together all stakeholders from academia, Research and Development
organisations, and industry to foster the growth of the
discipline.The first international conference on ‘Mechanochemistry
and Mechanical Alloying (INCOME1992)’ was held in Koásice (Slovakia)
in 1992. This was followed by INCOME1997 in Novosibirsk (Russia),
INCOME2000 in Prague (Czech Republic); INCOME2003, in Braunschweig
(Germany), and INCOME2006 again in Novosibirsk. This is the first
time that a conference of INCOME repute is going to be held in
India, and in Jamshedpur.
Dr. T. Ramasami,
Secretary, Department of Science & Technology, Govt. of India will
be the chief guest. Prof. M. Senna, President , International
Mechanochemistry Association will give the conference lecture. In
addition to presentation of technical papers, scientific posters
will be displayed. An
exhibition has also been also organized where state of the art
milling devices and characterization equipments will be displayed.
Mechanochemistry
and mechanical activation have moved a long way and have evolved as
frontier areas of research and applications, during the last two to
three decades. Notable developments have taken place in terms of
scientific understanding and applications in diverse fields,
encompassing all facets of metallurgy including metal extraction,
alloying, composites; traditional and advanced ceramics processing;
paints, pigments and dyes; catalysis, pharmaceuticals, agriculture,
utilization of wastes, energy and environment, and many more.
Simultaneous developments have taken place in terms of
characterization techniques of activated solids; quantification and
control of activation processes; and mechanical activation devices
for specific needs, etc. The developments in the field of
mechanochemistry are unfolding at a rapid rate in terms of basic
science, range of applications, and their impact. While significant
advances are taking place in each of the application areas, e.g.
smart mechanochemistry, pharmaceuticals, etc., and call for periodic
review, the need for cross fertilization of concepts and ideas is
increasingly becoming apparent. The four day deliverables will
contain all facets of Mechanochemistry including basic science,
application to various areas, newer developments and devices, and
industrial applications.
Jamshedpur, 1st
December 2008
The Inaugural function
of the VIth International Conference on Mechanochemistry
and Mechanical Alloying (INCOME 2008) was organized by NML,
Jamshedpur today. Dr. T. Ramasami, Secretary, Department of Science
and Technology, Govt. of India was the Chief Guest of the ceremony.
About 200 delegates including 60 foreign scientists and researchers
are participating in the conference.
Prof. S. P. Mehrotra,
Director, National Metallurgical Laboratory and Chairman, INCOME
2008 welcomed all the delegates. He mentioned that Mechanochemistry
is an evolving discipline and talked about its fundamentals,
widening of applications and the newer equipment and devices used
for the purpose. In the presidential address Prof. Peter Balaz,
founding member of the International Mechanochemistry Association
highlighted the history of the International Mechanochemistry
Association, which was founded in 1988.
Dr. T. Ramasami,
Secretary, Department of Science and Technology, Govt. of India
delivered a talk on ‘Revealing Beauty and Wonders of Nano World’.
He said that Nature has employed several principles of mechano-chemistry
and nano- size materials and structures had always existed. Our
realization of the behavior of materials of nano size that has
excited the world and global expectations are very high. He also
talked upon the beauty and wonders of nano structures in collagen.
The natural nano sized structures like skin for perspiration and
transpiration, peacock feather for decoration and shells, bones for
protection and load bearing functions are yet to be replicated by
man kind.
Dr. Rakesh Kumar, Convenor, INCOME 2008 proffered the
vote of thanks at the conclusion of the ceremony
Jamshedpur, 2nd
December 2008
The
second day of INCOME 2008 included sessions in Mechanochemistry of
Macromolecules and Applications in Pharmaceuticals, Severe Plastic
Deformation and Friction Stir Welding, Mechanical Alloying and
Advanced Materials, Building Management and Environment Management
and Nano- Particles and Nano- Composites. The sessions were preceded
by the Plenary Session Special Lectures. A total number of 29 papers
presented today. About 167 delegates including 47 foreign
scientists and researchers had participated in the today’s session.
The
sessions of today were preceded by three Plenary Lectures:
“Ultrafine grained materials through mechanical processing: An
overview” presented by, Prof. K.A. Padmanabhan, Anna University,
“Mechanochemistry of macromolecules and applications to
pharmaceuticals: where are we now? “ presented by Dr. E. Boldyreva,
” Using mechanical properties of crystals to quantify intermolecular
interactions” presented by, Prof. G. R. Desiraju, University of
Hyderabad. Some of the other important papers were presented in
today’s sessions were as follows:
Dr. Ashwini Nangia, University of Hyderabad presented
“Cocrystal design for pharmaceutical forms”. He presented various
aspects of pharmaceutical cocrystals and polymorphs e.g.
development of new heterosynthons using strong hydrogen bond
recognition and selective pairing of donors and acceptors. Dr. C.
Malla Reddy, Indian Institute of Science Education and Research,
kolkata presented “ Structure–property correlations in
shearing, bending and brittle organic crystals”. Dr.K.G. Korolev,
Institute of Solid State Chemistry, Russia presented paper
“Cell wall transformation during mechanical activation”. Prof.
Indranil Manna, IIT, Kharagpur delivered a talk on
“Mechano-chemical synthesis of Al-based nanocrystalline/ amorphous
alloys for high specific strength applications” He threw light on
his current study devoted to synthesize Al65Cu20Ti15
and Al50Ti40Si10 alloys with
in-situ nanometric intermetallic precipitates and/or nano-oxide (TiO2)
dispersion by solid-state mechanical alloying route and consolidate
milled powder by different sintering methods. Dr. M. Besterci ,
Institute of Materials Research of Slovak Academy of Sciences,
Kosice, Slovak Republic delivered a talk on Mechanical
alloying of Al-C system. Dr. K. L. Murty, North Carolina State
University, USA presented “Creep behavior of ball-milled
nanocrystalline aluminum”. Dr. Debasish
Bhattacharjee, Tata Steel, Jamshedpur presented ”Nanofluids
as coolants: Applications in steel industries”. Dr. A.N. Streletskii,
N. N. Semenov Institute of Chemical Physics, Moscow
presented “Metal- oxidizer mechanoactivated energetic nano
composites" Kang-In Rhee, Resource
Recycling R&D Centre, Korea presented
"Recycling R&D program at the RRDC Korea”
A poster
session was organized today where about 35 posters were presented
Jamshedpur,
3rd December 2008
A total number
of 28 papers were presented on the third day of the VI International
Conference on Mechanochemistry and Mechanical Alloying (INCOME 2008)
. Today’s sessions included papers in the areas of Mechanochemistry
of Macromolecules and Applications in Pharmaceuticals, Advance
Ceramics Science and Technology, Mechanical Alloying and Advanced
Materials, Mineral Processing and Extractive Metallurgy. The
sessions were preceded by the Plenary Session Special Lectures. “Plastic
deformation of fully dense Nanocrystalline material” presented
by, Dr. H. J. Fecht, Werkstoffe der Elektrotechnik, Universität Ulm
Germany, “On the existence of dynamic critical points“
presented by Dr. J. Linol, Université de Rouen, France, ”Estimation
of mechanochemical effects in heterogeneous processes”,
presented by, Dr. G. Mulas,
Universitŕ di Sassari, Italy. Some of the important papers
presented in today’s sessions are as following:
Dr. T. P.
Shakhtshneider, Institute of Solid State Chemistry and
Mechanochemistry, Russia, presented “Mechanochemistry and
solubilization of drugs”. He explained about his dissolution studies
showing that in the case of mechanocomposites, the release rate and
solubility of meloxicam increased compared with those of the
physical mixtures of the components and pure crystalline drug. This
study will be potentially useful in improving the oral
bioavailability of poorly water-soluble drugs. Dr. T. T. Friščić,
University of Cambridge, Cambridge presented the paper
“Development of liquid- assisted grinding for the synthesis of
hydrogen-bonded and coordination frameworks”. He highlighted that
the application of mechanosynthesis to the construction of
non-covalent e.g. hydrogen or halogen bonds between molecules has
been significantly improved by introducing a small amount of a
liquid phase into the mechanochemical reaction mixture. He also
talked about the recent discovery of molecular templating during
LAG, which has added an additional level of control to
mechanochemical synthesis of soft materials. The talk delivered by
Dr. B. S. Murty, Indian Institute of Technology, Chennai,
threw light on high energy ball milling that has established itself
as a viable and versatile route for the synthesis of nano materials.
His presentation dealt with the synthesis and properties of nano
materials prepared by high energy ball milling. Dr. N. K.
Mukhopadhyay, Banaras Hindu University, Varanasi, presented
“Synthesis of Nanocrystalline and amorphous phases in complex
metallic alloys during mechanical miling”. He said about the
Metal matrix composite (MMC) technology, which significantly
improves the wear resistance, elastic modulus and tensile strength
of unreinforced metals and alloys. In his paper a novel and
cost-effective processing route for in situ synthesis of TiC
particulates utilizing the self-propagating high-temperature
synthesis reaction of Al–Ti–C performs in molten magnesium was
investigated.
Dr. N. Kosenko,
Ivanovo State University of Chemical Technology, Russia,
presented “The mechanical treatment as a method of substances
passivation”, Dr. A. Politov, Institute of Solid State Chemistry
and Mechanochemistry SB RAS, Novosibirsk presented “Dimerization
of anthracene and relatedsubstances in diamond anvils and glass
mill”, Dr. Sh.Raygan, University of Tehran presented “Effect
of mechanical activation on the in-situ production of Fe-TiC
composite”, Dr. Projjal Basu, Universiti Sains Malaysia,
Malaysia presented “Synthesis of nanostructured titanium carbide
from Titanium oxide and Ferrotitanium through mechanical
activation”, Dr. T. Mousavi, Isfahan University of Technology,
Iran presented “The effect of Al2O3 content on the formation
mechanism and properties of NiTi-Al2O3 nano composite synthesized by
mechanical alloying”, Dr. Bassin Marc,
Thermo Fisher Scientific SARL, Switzerland
presented the paper “Integrated
automation solutions for top analytical performance and maximum
efficiency”, Dr. M.S. Senthil Saravanan, National Institute of
Technology, Tiruchirappalli presented “Influence of micro
and nanocrystalline powdermatrix on mechanical properties of CNT
reinforced Al-matrix composites, Dr. N. Kosova, Institute of
Solid State Chemistry and Mechanochemistry SB RAS, Novosibirs
presented “New composite ‘nano-micro’ cathode materials for
lithium-ion batteries prepared via mechanochemical route”, Dr.
T.Rojac Jozef Stefan Institute, Ljubljana, presented “Mechanochemical
synthesis of NaNbO3: a study of the reaction mechanism”, Dr. I.
Konstanchuk, Institute of Sold State Chemistry and
Mechanochemistry, Russia, presented “ Mechanically
alloyed magnesium-based materials for hydrogen storage and Dr. O.S.
Morozova, Institute of Chemical Physics RAS, Russia, presented “Stimulating
effect of boron admixture on hydrogen sorption-desorption properties
of mechanically activated Titanium”.
Some other
important invited papers presented in today’s session were
“Mechanochemical reactions of clay minerals with CsCI” presented by
Dr. S. Yariv, the Hebrew University of Jerusalem,
Jerusalem,
”Theoretical and application aspects concerning material treatment
in the Dynamic type mills”
by Dr. T. A.
Ketegenov, National Engineering Academy of the Republic of
Kazakhstan, Kazakhstan.
In the poster
session about 35 posters were presented.
Jamshedpur, 4th
December 2008
The fourth day of the VIth
International Conference On Mechanochemistry and Mechanical Alloying
(INCOME 2008) included sessions in Mechanical Alloying and Advanced
Materials, and Advance Ceramics Science and Technology. The sessions
were preceded by the Plenary Session Special Lectures. A total
number of 11 papers were presented today. The sessions of today were
preceded by three Plenary Lectures: “Glass formation” presented by,
Prof.P.Ramachandra Rao, “Local structure and size- dependent
properties of nanooxides prepared by mechanochemical routes“
presented by Dr. V. Šepelák, Braunschweig University
of Technology, Germany , and ” Specifics of mechanically driven
atomic distributions in interstitial alloys” presented by, Dr. J.
Foct, Université de Lille. Some of the important papers
presented in today’s sessions are as follows:
Dr. S. Srikanth, National
Metallurgical Laboratory Madras Centre, Chennai presented “Where
does the energy go in high energy milling?. He highlighted that for
understanding the magnitude and timescales of the temperature rise
during the high energy milling process, a study was undertaken using
low melting metals and alloys. The experimentally determined
crystallite size and strain correlated well with the values
estimated from line broadening analysis. Conversely, the
experimental melting point depression due to strain correlated well
with the theoretical calculations. Dr. P.C. Angelo, PSG College
of Technology, Coimbatore, presented “Hot isostatic
pressing of yttria dispersed 9Cr martensitic steel synthesized by
mechanical alloying”. He described the synthesis of ODS 9Cr
Martensitic steel by Mechanical Alloying of elemental metal
precursors. Nanocrystalline yttria used as the dispersoid was
synthesized via an efficient and economic Sol-Gel method. Dr. S.
Tikhov, Boreskov Institute of Catalysis., presented “Design
of the composite porous cermets synthesized through mechanical
alloying of Cr-Al powder followed by hydrothermal treatment and
calcination” . He focused that the cermet monoliths have
sufficiently high mechanical strength (up to ~20 MPa) and porosity
(35-57 %) with large pores (1-10
mm)
to be used as catalyst and membrane supports. The evolution of
microstructure with the Cr-Al powder alloying time had been
discussed. Dr. P.Brahma,
Gurudas College,Kolkata,
presented “Novel transport properties of nanostructured ferric
oxide“ He highlighted that the resistivity variation of the
unmilled sample can be ascribed to typical band conduction. The
resistivity decreases substantially with the progress of ball
milling. A decrease of about two orders of magnitude of resistivity
was observed for the specimen ball milled for 10h.It is clearly
observed that the resistivity variation of the Two activated
processes were observed with activation energies of
~0.06
and
~0.7eV,
respectively. Large and small particle sizes are responsible for the
two activation energies.
Dr. P. P. Chattopadhyay, Bengal
Engineering and Science University, Shibpur,
presented “Blue-violate photoluminescence from colloidal suspension
of nanocrystalline silicon-silicon oxide matrix prepared by ball
milling” He said that the intense violet-blue emission from nc-Si in
Si-oxide matrix prepared by chemically induced oxidation of
mechanically milled Si. Si powder was used as starting materials. He
also mentioned that there had been no previous report on blue PL
from nc-Si prepared by ball milling. The novel and inexpensive
synthesis route of nc-Si in oxide matrix, exhibiting blue-violet PL,
will open up a huge scope for potential applications. Dr. A.
Radhika
Devi,
Indian Institute of Technology, Chennai
presented
“Effect of surfactant addition on magnetic properties of Fe3O4
nanoparticles by ball milling” She said that, Magnetite nano
particles were synthesized in the presence of starch as surfactant
by ball milling for 30 hours in toluene medium. The amount of
surfactant addition was varied (8 wt %, 9 wt %,10 wt% ,11 wt % and
12 wt %) to study the variation of structural and magnetic
properties with surfactant content.